Testing standard
Dentistry — Base polymers — Part 1: Denture base polymers
Written and technically reviewed by Dak System Inc. engineeringLast reviewed
ISO 20795-1 specifies requirements for denture base polymers, including flexural strength and flexural modulus measured in three-point bending with the specimen in water at 37 °C. The limits depend on material type: flexural strength of at least 65 MPa for Types 1, 3, 4 and 5, and at least 60 MPa for Type 2, with modulus limits of 2000 MPa and 1500 MPa respectively.
From the test method to your testing system
Explore the DAK machines already listed for ISO 20795-1, then review the grips, measurement and setup requirements below.
Universal Testing MachineSeries 7200Explore the machine →
Universal Testing MachineSeries 9000Explore the machine →01Understand the method
Rectangular bars are prepared from the denture base material by its own processing route, finished along their length, measured individually and conditioned in water at 37 °C. Each bar is then loaded to fracture in a three-point bend fixture on a 50 mm span, at a crosshead speed of 5 mm/min ± 1 mm/min (0.20 in./min ± 0.04 in./min), with the specimen immersed at 37 °C. Flexural strength is calculated from the maximum force and flexural modulus from the initial straight portion of the load-deflection curve. Both come from the same trace on the same bar, so a specimen lost to a preparation fault costs both results, not one.
Whether a denture base will survive being bitten on. The limits are type-dependent: Types 1, 3, 4 and 5 must reach at least 65 MPa flexural strength and 2000 MPa flexural modulus, while Type 2 — the autopolymerised group — must reach 60 MPa and 1500 MPa. The lower Type 2 requirements are not a concession but a recognition that autopolymerised materials polymerise less completely. The standard also sets limits on residual monomer, water sorption and solubility, so passing the bending requirements is necessary and not sufficient.
02Prepare the specimen and test settings
The type decides the limit. A bar that passes as a Type 2 material fails as a Type 1, and the type is a property of the product, not a choice made in the laboratory.
Flexural strength and modulus are only two of this standard's requirements. It also sets limits on residual monomer, water sorption and solubility, and a material that meets the bending limits has not thereby met the standard.
03Build the test setup on a DAK machine
Low force with good resolution, a crosshead holding 5 mm/min ± 1 mm/min, a bend fixture built to the standard's dimensions, and 37 °C water around the specimen for the whole test. A denture base bar commonly fractures under 200 N, so the load cell has to be chosen for the specimen. The geometry is fixed by the method rather than chosen by the operator: a bar 64 mm long, 10,0 mm ± 0,2 mm wide and 3,3 mm ± 0,2 mm high, loaded centrally on 3,2 mm diameter anvils set 50 mm apart. That matters because the acceptance limits are quoted against that geometry and that speed — a longer span, or a faster crosshead on a viscoelastic acrylic, produces a different calculated strength from the same material.
A three-point bend fixture with the span and roller diameters the standard sets. Denture base bars are small and the span tolerance is tight — this is a fixture built to the method's dimensions, not a general-purpose jig set by eye.
Specifications
The test is run with the specimen in water at 37 °C. A bath or conditioning arrangement holding that temperature around the specimen is part of the test, not an optional extra.
SpecificationsDak verifies against whichever standard the method names, and where a class applies our frames sit a class tighter than it asks.
| The method asks for | Dak supplies | |
|---|---|---|
| Capacity | Low — a denture base bar in three-point bending commonly breaks under 200 N | Load cells from 1 kg to 60 ton on the Series 7200, and 0.5 to 100 kN on the Series 9000 |
| Force accuracy | ISO 7500-1 Class 1 | ISO 7500-1 Class 0.5 — a class tighter than the method asks |
| Gripping | A three-point bend fixture to the dimensions the standard specifies, used with the specimen immersed in water at 37 °C | Our bend fixtures, built to the specimen |
| Environment | Immersed in water at 37 °C | 3009 series chambers, −150 °C to +400 °C — temperature only |
04Run the test
05Calculate, report and interpret
σ = 3FL / (2bh²)
Height is squared, so a measurement error there is doubled in the result. Measure each bar rather than assuming the mould.
E = F₁L³ / (4bh³d₁)
Taken from the initial straight portion. Reading it across a curved region gives a modulus that is not one.
65 MPa and 2000 MPa; 60 MPa and 1500 MPa for Type 2
Heat-cured materials polymerise more completely than autopolymerised ones, and the requirements follow that reality rather than pretending otherwise.
Testing dry, which raises the numbers and describes a condition the appliance is never in. Setting the span by eye rather than to the specified value. Reading the modulus across a curved part of the trace instead of the initial straight portion. Assuming the mould's nominal dimensions rather than measuring each bar, when height is squared in the arithmetic. Comparing a result against the wrong type's limits. And accepting a bar that fractured from a visible void, which reports a moulding fault as a material property rather than rejecting it and recording why.
06Compare methods and find answers
| ISO 20795-1 | ISO 20795-2 | |
|---|---|---|
| Covers | Denture base polymers | Orthodontic base polymers |
| Property | Flexural strength and modulus, plus monomer, sorption and solubility | The equivalent requirements for its own materials |
| Tested | In water at 37 °C | In water at 37 °C |
| Cite | For denture bases | For orthodontic appliances |
They are two parts of one standard covering two different product groups. The bending geometry is shared, but the material types and the limits are not, and a certificate must name the part that applies to the appliance.
ISO 20795-1:2013 is the international standard for denture base polymers. It specifies requirements for the materials used to make the pink acrylic body of a denture, including flexural strength and flexural modulus measured in three-point bending, along with limits on residual monomer, water sorption and solubility. Meeting the bending limits alone does not satisfy the standard.
For Types 1, 3, 4 and 5 the flexural strength must be at least 65 MPa and the flexural modulus at least 2000 MPa. For Type 2, the autopolymerised group, the limits are 60 MPa and 1500 MPa. The lower figures reflect the fact that autopolymerised materials polymerise less completely than heat-cured ones, and the standard sets its requirements against that rather than around it.
Because that is the condition a denture works in. Acrylic absorbs water, and absorbed water plasticises the polymer and lowers both its strength and its stiffness. A bar tested dry in a laboratory at room temperature gives a higher number that describes a state the appliance is never in. Testing immersed at body temperature is what makes the limits mean something clinically.
Because a void near the tensile face of a bar in bending is a fracture origin, and the specimen breaks from it at a load well below what the material would otherwise carry. The result then describes the processing of that particular bar rather than the material. Inspecting every bar before loading, and rejecting and recording any with visible voids, is what separates a material result from a moulding fault.
Because a transverse scratch on the tensile face is a notch, and acrylic is notch-sensitive. Finishing marks running across the bar concentrate stress exactly where bending puts the maximum tension, and the fracture initiates there. Finishing along the length leaves marks parallel to the tensile stress, where they do far less.
ISO/DIS 20795-1 is in development as a revision of the 2013 edition and introduces a further material type. Until it is published, ISO 20795-1:2013 remains the edition in force, and that is the one to cite on a certificate. Where a specification predates the revision, confirm which edition the customer is working to before testing.
A testing frame with low-force capability and good resolution — a denture base bar commonly breaks under 200 N — a crosshead holding 5 mm/min ± 1 mm/min, a three-point bend fixture with 3,2 mm diameter anvils on a 50 mm span, and a means of holding the specimen in water at 37 °C throughout the test. The geometry is not adjustable to taste: the acceptance limits are quoted against that span and that speed, and changing either changes the calculated strength.
Discuss your specimen, test requirements and reporting needs with DAK engineering.
This page describes the method as practised. The governing text is the current edition from the issuing body. Tell us what you are testing and we will answer with the machine, the fixture and a quotation.
